A novel spectrophotometric method for determination of chloramphenicol based on diazotization reaction at room temperature
| Main Authors: | Wafi, Abdul, Supriyanto, Ganden, Tjahjandarie, Tjitjik Srie |
|---|---|
| Format: | Journal PeerReviewed Book |
| Bahasa: | eng |
| Terbitan: |
Gadjah Mada University
, 2016
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| Subjects: | |
| Online Access: |
http://repository.uin-malang.ac.id/840/1/1039-3318-1-PB.pdf http://repository.uin-malang.ac.id/840/ http://pdm-mipa.ugm.ac.id/ojs/index.php/ijc/article/view/1039 |
| ctrlnum |
840 |
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<dc schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/ http://www.openarchives.org/OAI/2.0/oai_dc.xsd"><relation>http://repository.uin-malang.ac.id/840/</relation><title>A novel spectrophotometric method for determination of chloramphenicol based on diazotization reaction at room temperature</title><creator>Wafi, Abdul</creator><creator>Supriyanto, Ganden</creator><creator>Tjahjandarie, Tjitjik Srie</creator><subject>030101 Analytical Spectrometry</subject><subject>030107 Sensor Technology (Chemical aspects)</subject><description>An analytical method for determination of chloramphenicol (CAP) based on the diazotization reaction at room temperature has been developed. The CAP was reduced using zinc powder (Zn) and diazotization reaction was carried out at room temperature in the presence of NaNO2, bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) as catalyst. 2-napthol was used as coupling agent to form a red-violet solution and the absorbance was measured by UV-Vis spectrophotometer at 554 nm. The optimization of analytical parameters including reducing agent, catalyst, coupling agent and time response were 0.15 g, 0.15 g, 230.67 μg/mL and 8-9 min respectively.</description><publisher>Gadjah Mada University</publisher><date>2016-03-01</date><type>Journal:Journal</type><type>PeerReview:PeerReviewed</type><type>Book:Book</type><language>eng</language><identifier>http://repository.uin-malang.ac.id/840/1/1039-3318-1-PB.pdf</identifier><identifier> Wafi, Abdul and Supriyanto, Ganden and Tjahjandarie, Tjitjik Srie (2016) A novel spectrophotometric method for determination of chloramphenicol based on diazotization reaction at room temperature. Indonesian Journal of Chemistry, 16 (1). pp. 32-35. ISSN 1411-9420 </identifier><relation>http://pdm-mipa.ugm.ac.id/ojs/index.php/ijc/article/view/1039</relation><recordID>840</recordID></dc>
|
| language |
eng |
| format |
Journal:Journal Journal PeerReview:PeerReviewed PeerReview Book:Book Book |
| author |
Wafi, Abdul Supriyanto, Ganden Tjahjandarie, Tjitjik Srie |
| title |
A novel spectrophotometric method for determination of chloramphenicol based on diazotization reaction at room temperature |
| publisher |
Gadjah Mada University |
| publishDate |
2016 |
| topic |
030101 Analytical Spectrometry 030107 Sensor Technology (Chemical aspects) |
| url |
http://repository.uin-malang.ac.id/840/1/1039-3318-1-PB.pdf http://repository.uin-malang.ac.id/840/ http://pdm-mipa.ugm.ac.id/ojs/index.php/ijc/article/view/1039 |
| contents |
An analytical method for determination of chloramphenicol (CAP) based on the diazotization reaction at room temperature has been developed. The CAP was reduced using zinc powder (Zn) and diazotization reaction was carried out at room temperature in the presence of NaNO2, bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) as catalyst. 2-napthol was used as coupling agent to form a red-violet solution and the absorbance was measured by UV-Vis spectrophotometer at 554 nm. The optimization of analytical parameters including reducing agent, catalyst, coupling agent and time response were 0.15 g, 0.15 g, 230.67 μg/mL and 8-9 min respectively. |
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IOS3710.840 |
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Universitas Islam Negeri Maulana Malik Ibrahim Malang |
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onesearch.perpusnas.go.id mill.onesearch.id fkp2tn.onesearch.id ptki.onesearch.id |
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114 |
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library:university library |
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Perpustakaan UIN Maulana Malik Ibrahim Malang |
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504 |
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Research Repository UIN Maulana Malik Ibrahim Malang |
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3710 |
| subject_area |
Engineering/Ilmu Teknik Islam and Social Sciences/Islam dan Ilmu-ilmu Sosial |
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MALANG |
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JAWA TIMUR |
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IOS3710 |
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2016-11-25T06:56:18Z |
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2022-10-21T08:08:44Z |
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17.203468 |