SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED PALM KERNEL SHELL WASTE WITH FE3O4

Main Authors: Widyaningrum, Bernadeta Ayu, Apriani, Dita, Amanda, Putri, Ismadi, Ismadi, Sutanto, Sutanto
Format: Article info application/pdf eJournal
Bahasa: eng
Terbitan: Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency , 2021
Subjects:
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fullrecord <?xml version="1.0"?> <dc schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/ http://www.openarchives.org/OAI/2.0/oai_dc.xsd"><title lang="en-US">SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED PALM KERNEL SHELL WASTE WITH FE3O4</title><creator>Widyaningrum, Bernadeta Ayu</creator><creator>Apriani, Dita</creator><creator>Amanda, Putri</creator><creator>Ismadi, Ismadi</creator><creator>Sutanto, Sutanto</creator><subject lang="en-US">Palm Kernel Shell, Hummer Method, Graphene Oxide, GO-Fe3O4 Composite, Co-Precipitation</subject><description lang="en-US">SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED&#xA0;PALM KERNEL SHELL WASTE WITH Fe3O4. In this study, GO-Fe3O4 were fabricated by co-precipitation technique and the graphene oxide (GO) were synthesized from an agricultural biomass, palm kernel shell, via Hummer&#x2019;s method. Field Emission Scanning Electron Microscopy and Energy Dispersive Spectrum (FESEM-EDS), Fourier Transform Infra-Red (FT-IR) spectroscopy, X-Ray Diffractometer (XRD), and Raman spectroscopy were used to analysis the successful attachment of&#xA0;Fe3O4 onto the surface of GO. Morphology observation showed that&#xA0;Fe3O4 were heterogeneously deposited on the surface of GO. FT-IR spectra shows peak that incorporated to oxygenated functional groups and sharp peak at 586&#xA0;cm-1 confirmed to lattice absorption of Fe3O4. The percentage of composition of GO-Fe3O4 was characterized by energy dispersive spectroscopy and the results also confirmed in XRD exhibits similar properties with JCPDS 19-0629 for magnetite more dominant than GO. From Raman spectroscopy analysis shows that 1343.82 cm-1&#xA0;(D-band) and 1584.62&#xA0;cm-1 (G-band) and 2698&#xA0;cm-1 (2D-band) indicates GO and GO-Fe3O4 were successfully synthesized.</description><publisher lang="en-US">Center for Science &amp; Technology of Advanced Materials - National Nuclear Energy Agency</publisher><contributor lang="en-US"/><date>2021-08-16</date><type>Journal:Article</type><type>Other:info:eu-repo/semantics/publishedVersion</type><type>Other:</type><type>File:application/pdf</type><type>File:application/pdf</type><identifier>http://jurnal.batan.go.id/index.php/jsmi/article/view/6310</identifier><identifier>10.17146/jsmi.2021.22.3.6310</identifier><source lang="en-US">Jurnal Sains Materi Indonesia; Vol 22, No 2: APRIL 2021; 101 - 109</source><source lang="id-ID">Jurnal Sains Materi Indonesia; Vol 22, No 2: APRIL 2021; 101 - 109</source><source>2614-087X</source><source>1411-1098</source><language>eng</language><relation>http://jurnal.batan.go.id/index.php/jsmi/article/view/6310/pdf</relation><relation>http://jurnal.batan.go.id/index.php/jsmi/article/view/6310/pdf_1</relation><rights lang="en-US">Copyright (c) 2021 Jurnal Sains Materi Indonesia</rights><rights lang="en-US">http://creativecommons.org/licenses/by-nc-sa/4.0</rights><recordID>article-6310</recordID></dc>
language eng
format Journal:Article
Journal
Other:info:eu-repo/semantics/publishedVersion
Other
Other:
File:application/pdf
File
Journal:eJournal
author Widyaningrum, Bernadeta Ayu
Apriani, Dita
Amanda, Putri
Ismadi, Ismadi
Sutanto, Sutanto
title SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED PALM KERNEL SHELL WASTE WITH FE3O4
publisher Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency
publishDate 2021
topic Palm Kernel Shell
Hummer Method
Graphene Oxide
GO-Fe3O4 Composite
Co-Precipitation
url http://jurnal.batan.go.id/index.php/jsmi/article/view/6310
http://jurnal.batan.go.id/index.php/jsmi/article/view/6310/pdf
http://jurnal.batan.go.id/index.php/jsmi/article/view/6310/pdf_1
contents SYNTHESIS AND CHARACTERIZATION: COMPOSITE OF GRAPHENE OXIDE BASED PALM KERNEL SHELL WASTE WITH Fe3O4. In this study, GO-Fe3O4 were fabricated by co-precipitation technique and the graphene oxide (GO) were synthesized from an agricultural biomass, palm kernel shell, via Hummer’s method. Field Emission Scanning Electron Microscopy and Energy Dispersive Spectrum (FESEM-EDS), Fourier Transform Infra-Red (FT-IR) spectroscopy, X-Ray Diffractometer (XRD), and Raman spectroscopy were used to analysis the successful attachment of Fe3O4 onto the surface of GO. Morphology observation showed that Fe3O4 were heterogeneously deposited on the surface of GO. FT-IR spectra shows peak that incorporated to oxygenated functional groups and sharp peak at 586 cm-1 confirmed to lattice absorption of Fe3O4. The percentage of composition of GO-Fe3O4 was characterized by energy dispersive spectroscopy and the results also confirmed in XRD exhibits similar properties with JCPDS 19-0629 for magnetite more dominant than GO. From Raman spectroscopy analysis shows that 1343.82 cm-1 (D-band) and 1584.62 cm-1 (G-band) and 2698 cm-1 (2D-band) indicates GO and GO-Fe3O4 were successfully synthesized.
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