Fabrication and Characterization of Organoclay Reinforced Polyester Based Hybrid Nanocomposite Materials

Main Authors: Zaman, Noor, Ahmed, Shfique, Sanaullah, Muhammad, Rehman, Attique Ur, Shar, Abdul Raheem, Luhur, Muhammad Ramzan
Format: Article
Bahasa: eng
Terbitan: , 2018
Subjects:
Online Access: https://zenodo.org/record/1400626
ctrlnum 1400626
fullrecord <?xml version="1.0"?> <dc schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/ http://www.openarchives.org/OAI/2.0/oai_dc.xsd"><creator>Zaman, Noor</creator><creator>Ahmed, Shfique</creator><creator>Sanaullah, Muhammad</creator><creator>Rehman, Attique Ur</creator><creator>Shar, Abdul Raheem</creator><creator>Luhur, Muhammad Ramzan</creator><date>2018-06-20</date><description>Synthesis and characterization of polyester nanocomposites was conducted in order to fabricate hybrid composite materials of polyester/montmorillonite (MMT). Polyester based polymeric nanocomposite materials were synthesized by incorporating MMT nanoclay to produce polyester/MMT hybrid materials. Successful efforts were made to fabricate hybrid nanocomposite materials based on matrix (polyester based) and reinforcement (organoclay) through sonication at 6 and 12 hours. Synthesized nanocomposite polymers (polyester/MMT) showed different properties when compared to the properties of MMT and polyester, which confirmed the successful fabrication of the desired material. The finest incorporation of polyester with MMT was verified by UVVisible spectrophotometer, Fourier tranform-infrared (FTIR) and scanning electron microscopy (SEM). The disappearance of the Si-O characteristic peak was observed in the FTIR spectrum justifying the fabrication of the desired composite materials. Colored SEM images were used to confirm the fine homogenous distribution of organoclay. Black SEM images showed the matrix and reinforcement together. SEM, FTIR and UV-Visible spectroscopic techniques were used to analyze polyester based nanocomposite materials and organoclay was found randomly distributed in the polymeric matrix whereas on the surface was observed to be mostly uniform.</description><identifier>https://zenodo.org/record/1400626</identifier><identifier>10.5281/zenodo.1400626</identifier><identifier>oai:zenodo.org:1400626</identifier><language>eng</language><relation>doi:10.5281/zenodo.1400625</relation><relation>url:https://zenodo.org/communities/etasr</relation><rights>info:eu-repo/semantics/openAccess</rights><rights>https://creativecommons.org/licenses/by/4.0/legalcode</rights><source>Engineering, Technology &amp; Applied Science Research 8(3) 3038-3040</source><subject>polyester</subject><subject>nanocomposite</subject><subject>reinforcement</subject><subject>UV-Visible spectrophotometer</subject><title>Fabrication and Characterization of Organoclay Reinforced Polyester Based Hybrid Nanocomposite Materials</title><type>Journal:Article</type><type>Journal:Article</type><recordID>1400626</recordID></dc>
language eng
format Journal:Article
Journal
author Zaman, Noor
Ahmed, Shfique
Sanaullah, Muhammad
Rehman, Attique Ur
Shar, Abdul Raheem
Luhur, Muhammad Ramzan
title Fabrication and Characterization of Organoclay Reinforced Polyester Based Hybrid Nanocomposite Materials
publishDate 2018
topic polyester
nanocomposite
reinforcement
UV-Visible spectrophotometer
url https://zenodo.org/record/1400626
contents Synthesis and characterization of polyester nanocomposites was conducted in order to fabricate hybrid composite materials of polyester/montmorillonite (MMT). Polyester based polymeric nanocomposite materials were synthesized by incorporating MMT nanoclay to produce polyester/MMT hybrid materials. Successful efforts were made to fabricate hybrid nanocomposite materials based on matrix (polyester based) and reinforcement (organoclay) through sonication at 6 and 12 hours. Synthesized nanocomposite polymers (polyester/MMT) showed different properties when compared to the properties of MMT and polyester, which confirmed the successful fabrication of the desired material. The finest incorporation of polyester with MMT was verified by UVVisible spectrophotometer, Fourier tranform-infrared (FTIR) and scanning electron microscopy (SEM). The disappearance of the Si-O characteristic peak was observed in the FTIR spectrum justifying the fabrication of the desired composite materials. Colored SEM images were used to confirm the fine homogenous distribution of organoclay. Black SEM images showed the matrix and reinforcement together. SEM, FTIR and UV-Visible spectroscopic techniques were used to analyze polyester based nanocomposite materials and organoclay was found randomly distributed in the polymeric matrix whereas on the surface was observed to be mostly uniform.
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