Åkermanite glass microspheres: Preparation and perspectives of sinter- crystallization

Main Authors: Dasan A., Talimian A., Kraxner J., Galusek D., Elsayed H., Bernardo E.
Format: Article Journal
Bahasa: eng
Terbitan: , 2021
Subjects:
Online Access: https://zenodo.org/record/4916437
ctrlnum 4916437
fullrecord <?xml version="1.0"?> <dc schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/ http://www.openarchives.org/OAI/2.0/oai_dc.xsd"><creator>Dasan A.</creator><creator>Talimian A.</creator><creator>Kraxner J.</creator><creator>Galusek D.</creator><creator>Elsayed H.</creator><creator>Bernardo E.</creator><date>2021-05-21</date><description>Glass microspheres with the exact stoichiometry of &#xE5;kermanite (Ca2MgSi2O7), one of the most promising modern bioceramics, were produced by the flame synthesis method. The distinctive high cooling rate was found to prevent the crystallization; the size of amorphous microbeads could be correlated with the size of partially crystal-lized precursor powders, deriving from conventional melt quenching and milling. The glass microspheres were characterized in terms of crystallization and sintering behav-ior, in the perspective of applications in additive manufacturing of &#xE5;kermanite- based scaffolds. The results showed that merwinite (Ca3MgSi2O8) is the primary product of glass devitrification; only in a second stage, merwinite reacts with the residual glass and yields &#xE5;kermanite. The rapid crystallization, implying limited viscous flow sintering, was tested as an opportunity to create components with complex porosity distribution.</description><identifier>https://zenodo.org/record/4916437</identifier><identifier>10.5281/zenodo.4916437</identifier><identifier>oai:zenodo.org:4916437</identifier><language>eng</language><relation>info:eu-repo/grantAgreement/EC/H2020/739566/</relation><relation>doi:10.5281/zenodo.4916436</relation><relation>url:https://zenodo.org/communities/funglass</relation><rights>info:eu-repo/semantics/openAccess</rights><rights>https://creativecommons.org/licenses/by/4.0/legalcode</rights><source>International Journal of Glass Applied Science special issue(Special Issue)</source><subject>additive manufacturing, &#xE5;kermanite, crystallization, glass microspheres, viscous flow sintering</subject><title>&#xC5;kermanite glass microspheres: Preparation and perspectives of sinter- crystallization</title><type>Journal:Article</type><type>Journal:Article</type><recordID>4916437</recordID></dc>
language eng
format Journal:Article
Journal
Journal:Journal
author Dasan A.
Talimian A.
Kraxner J.
Galusek D.
Elsayed H.
Bernardo E.
title Åkermanite glass microspheres: Preparation and perspectives of sinter- crystallization
publishDate 2021
topic additive manufacturing
åkermanite
crystallization
glass microspheres
viscous flow sintering
url https://zenodo.org/record/4916437
contents Glass microspheres with the exact stoichiometry of åkermanite (Ca2MgSi2O7), one of the most promising modern bioceramics, were produced by the flame synthesis method. The distinctive high cooling rate was found to prevent the crystallization; the size of amorphous microbeads could be correlated with the size of partially crystal-lized precursor powders, deriving from conventional melt quenching and milling. The glass microspheres were characterized in terms of crystallization and sintering behav-ior, in the perspective of applications in additive manufacturing of åkermanite- based scaffolds. The results showed that merwinite (Ca3MgSi2O8) is the primary product of glass devitrification; only in a second stage, merwinite reacts with the residual glass and yields åkermanite. The rapid crystallization, implying limited viscous flow sintering, was tested as an opportunity to create components with complex porosity distribution.
id IOS16997.4916437
institution ZAIN Publications
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library Cognizance Journal of Multidisciplinary Studies
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collection Cognizance Journal of Multidisciplinary Studies
repository_id 16997
subject_area Multidisciplinary
city Stockholm
province INTERNASIONAL
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repoId IOS16997
first_indexed 2022-06-06T04:15:49Z
last_indexed 2022-06-06T04:15:49Z
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